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Which guidelines apply to NMR sample preparation?

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Which guidelines apply to NMR sample preparation?

Ensure the solution (within the region of the RF coils ) is clear and homogeneous.

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Use a sample depth gauge.

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Use 5 mm NMR tubes: 7 inches or 8 inches.

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Solubility in deuterated solvent is key factor in solvent choice

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Dissolve the sample in a non-deuterated solvent.

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