After calibrating axis, Use the “Integrate” option to identify peak positions for all proton and carbon 1D

Type “efp” 1st to perform a Fourier transform

After calibrating axis, Use the “Pick Peaks” option to identify peak positions for all proton and carbon 1D

Type “apk” 2nd for automatic phase correction

Type 'abs' 3rd for automatic baseline correction

Type “rga” to adjust receiver gain

Type “efp” after all other processing commands to perform a Fourier transform

You must book time using the room/location 8-419 NMR.

You must book time using the "All Day Booking" feature on the 8-419 300 NMR calendar.

You must complete the Chemistry Department Instrument Acknowledgement Form before booking.

you must fill out the paper sign-up sheet in the NMR room (8-419).

You can conduct experiments without formal training as long as you book time.

You must be trained by a Faculty member or the Chemistry Technician (Chemtech) and pass a short practical test before booking.

efp

zg

rga

edc

"Lift" on BSMS control panel OR commandline 'ej' for air up and 'ij' for air down.

Manual lever.

Hydraulic lift.

Air lift system.

Poor shimming reduces resolution

Locking adjusts to deuterium signals

Locking and shimming are done before running any experiment

Locking is unnecessary for carbon-13 NMR

Shimming corrects magnetic field gradients.

They reduce interference with sample signals.

They increase the boiling point of the sample.

They are non-hygroscopic.

They provide a deuterium lock signal.